J Adhes Dent 21 (2019), No. 6 6. Dec. 2019
J Adhes Dent 21 (2019), No. 6 (06.12.2019)
Page 509-516, doi:10.3290/j.jad.a43610, PubMed:31802066
Influence of Monomer Systems on the Bond Strength Between Resin Composites and Polymerized Fiber-Reinforced Composite upon Aging
Khan, Aftab A. / Mohamed, Badreldin A. / Al-Shamrani, Sultan Saleh / Ramakrishnaiah, Ravikumar / Perea-Lowery, Leila / Säilynoja, Eija / Vallittu, Pekka K.
Purpose: This study examined the influence of different monomer systems on the tensile bond strength between a resin composite and a polymerized fiber-reinforced composite (FRC). The influence of the age (shelf-life) of the FRC prepreg (reinforcing fiber pre-impregnated with a resin system) before preparing the FRC substrate for the bonding test was also assessed.
Materials and Methods: Semi-interpenetrating polymer network (semi-IPN)-based glass FRC prepregs were aged for various durations (1, 1.5, and 3 years) at 4°C before being used to prepare FRC substrates via light polymerization. Four groups of aged prepregs were prepared through different treatments with: 1. no primer; 2. a dimethacrylate-based adhesive primer; 3. a universal primer; and 4. a specific composite primer. Subsequently, a resin composite luting cement was applied on the treated FRC substrates and cured with light. The water sorption of the FRC-composite specimens was determined. Then, the differences in the tensile bond strength were evaluated using ANOVA (p ≤ 0.05).
Results: There were signiﬁcant differences in the tensile bond strength between the composite cement and the FRC according to the primer used (p < 0.001), aging time (p < 0.001), and their interactive effect (p < 0.001).
Conclusion: The monomers of the universal primer demonstrated the best ability to diffuse into the semi-IPN structure of the polymer matrix of FRC. This improved the interfacial bond strength between the composite cement and the FRC substrate.
Keywords: adhesive interface, fiber-reinforced composite, poly(methyl methacrylate), primer, semi-interpenetrating polymer network, tensile bond strength